A simple protocol for determining the zone axis direction from selected-area electron diffraction spot patterns of cubic materials

Journal of Applied Crystallography, vol. 57, pp. 1263–1269

Abstract

Using the well known R n ratio method, a protocol has been elaborated for determining the lattice direction for the 15 most common cubic zone axis spot patterns. The method makes use of the lengths of the three shortest reciprocal-lattice vectors in each pattern and the angles between them. No prior pattern calibration is required for the method to work, as the R n ratio method is based entirely on geometric relationships. In the first step the pattern is assigned to one of three possible pattern types according to the angles that are measured between the three reciprocal-lattice vectors. The lattice direction [ uvw ] and possible Bravais type(s) and Laue indices of the corresponding reflections can then be determined by using lookup tables. In addition to determining the lattice direction, this simple geometric analysis allows one to distinguish between the P , I and F Bravais lattices for spot patterns aligned along [013], [112], [114] and [233]. Moreover, the F lattice can always be uniquely identified from the [011] and [123] patterns.

Authors 1

1. Thomas E. Weirich corresponding Aachen Gemeinschaftslabor für Elektronenmikroskopie (GFE)

   RWTH Aachen University

   Affiliation as printed

   Gemeinschaftslabor für Elektronenmikroskopie (GFE) RWTH Aachen University Ahornstrasse 55 52074Aachen Germany

   Gemeinschaftslabor für Elektronenmikroskopie (GFE), RWTH Aachen University, Ahornstrasse 55, 52074 Aachen, Germany